Síntesis y caracterización de nanopartículas de oro en solución utilizando quitosán como agente reductor
Synthesis and characterization of gold nanoparticles in solution using chitosan as reducing agent
Barra lateral del artículo
Ver / Descargar
PDF (English)
FLIP
(English)
HTML (English)
Cómo citar
Flórez Barajas, F. J. ., Sánchez Acevedo, Z. C., & Peña Pedraza , H. . (2019). Síntesis y caracterización de nanopartículas de oro en solución utilizando quitosán como agente reductor. Respuestas, 24(2), 49–55. https://doi.org/10.22463/0122820X.1830
Más formatos de cita
Número
Sección
Artículos de investigación
Términos de la licencia
(VER)
Contenido principal del artículo
Resumen
En la actualidad las nanopartículas metálicas, en especial, las de metales nobles como el oro, han cobrado importancia debido a sus potenciales aplicaciones en diversas ramas, ya que sus propiedades fisicoquímicas y su bajo grado de toxicidad las convierten en materiales de gran importancia. En este trabajo, se realizó la síntesis de nanopartículas de oro en solución, utilizando como agente reductor la biomolécula quitosán. Además, las nanopartículas fueron caracterizadas por una técnica espectrofotométrica ultravioleta visible, para verificar la eficacia del proceso de síntesis. El espectro mostró que las nanopartículas sintetizadas presentan una banda de absorción centrada en 530 nm, característica propia de partículas de oro de tamaño nanométrico.
Palabras clave
Descargas
Los datos de descargas todavía no están disponibles.
Detalles del artículo
Referencias
Taniguchi, N., On the Basic Concept of Nanotechnology, in Actas de la ICPE (InternationalConference on Production Eng. 1974: Tokio. p. 18-23.
Sant, S.B., Nanoparticles: From Theory to Applications. Materials and Manufacturing Processes, 2012. 27(12): p. 1462-1463.
Ball, P., Natural strategies for the molecular engineer. Nanotechnology, 2002. 13: p. 15-28.
Brock, S.L., Nanostructures and Nanomaterials: Synthesis, Properties and Applications By Guozhang Cao (University of Washington). Imperial College Press (distributed by World Scientific): London. Journal of the American Chemical Society, 2004. 126(44): p. 14679-14679.
Velásquez, C., S. Koteich, and F. López, Nanopartículas: Fundamentos y Aplicaciones. Universidad de Los Andes, Mérida, Venezuela., 2015.
Bönnemann, H. and Ryan M. Richards, Nanoscopic Metal Particles − Synthetic Methods and Potential Applications. European Journal of Inorganic Chemistry, 2001. 2001(10): p. 2455-2480.
Sifontes, A., et al., Preparación de nanopartículas de plata en ausencia de polimeros estabilizantes. Vol. 33. 2010.
Sperling, R.A. and W.J. Parak, Surface modification, functionalization and bioconjugation of colloidal inorganic nanoparticles. Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, 2010. 368(1915): p. 1333-1383.
Alivisatos, A.P., Semiconductor Clusters, Nanocrystals, and Quantum Dots. Science, 1996. 271(5251): p. 933-937.
Banin, U., et al., Identification of atomic-like electronic states in indium arsenide nanocrystal quantum dots. Nature, 1999. 400: p. 542.
Collier, C.P., et al., Reversible Tuning of Silver Quantum Dot Monolayers Through the Metal-Insulator Transition. Science, 1997. 277(5334): p. 1978-1981.
Kelly, K.L., et al., The optical properties of metal nanoparticles: The influence of size, shape, and dielectric environment. Journal of Physical Chemistry B, 2003. 107, No. 3: p. 668-677.
Pei, Y. and X.C. Zeng, Investigating the structural evolution of thiolate protected gold clusters from first-principles. Nanoscale, 2012. 4(14): p. 4054-4072.
Lv, Y., et al., Preparation of Dialdehyde Chitosan and its Application in Green Synthesis of Silver Nanoparticles. Vol. 8. 2013. 6161-6172.
Sarkany, A., et al., Unsupported Pd nanoparticles prepared by gamma-radiolysis of PdCl2. Solid State Ionics, 2005. 176, No. 1-2: p. 209–215.
G. Nanoparticles: From Theory to Application. 2004: WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Luo, C., et al., The role of poly (ethylene glycol) in the formation of silver nanoparticles. Journal of Colloid and Interface Science, 2005. 288(2): p. 444-448.
Pal, S., Y.K. Tak, and J.M. Song, Does the Antibacterial Activity of Silver Nanoparticles Depend on the Shape of the Nanoparticle? A Study of the Gram-Negative Bacterium em Escherichia coli/em. Applied and Environmental Microbiology, 2007. 73(6): p. 1712-1720.
Raveendran, P., J. Fu, and S.L. Wallen, A simple and “green” method for the synthesis of Au, Ag, and Au–Ag alloy nanoparticles. Green Chemistry, 2006. 8(1): p. 34-38.
Kapoor, S., Preparation, Characterization, and Surface Modification of Silver Particles. Langmuir, 1998. 14(5): p. 1021-1025.
Guozhong, C. Nanostructures and Nanomaterials Imperial College Press, 2004.
Sant, S.B., Nanoparticles: From Theory to Applications. Materials and Manufacturing Processes, 2012. 27(12): p. 1462-1463.
Ball, P., Natural strategies for the molecular engineer. Nanotechnology, 2002. 13: p. 15-28.
Brock, S.L., Nanostructures and Nanomaterials: Synthesis, Properties and Applications By Guozhang Cao (University of Washington). Imperial College Press (distributed by World Scientific): London. Journal of the American Chemical Society, 2004. 126(44): p. 14679-14679.
Velásquez, C., S. Koteich, and F. López, Nanopartículas: Fundamentos y Aplicaciones. Universidad de Los Andes, Mérida, Venezuela., 2015.
Bönnemann, H. and Ryan M. Richards, Nanoscopic Metal Particles − Synthetic Methods and Potential Applications. European Journal of Inorganic Chemistry, 2001. 2001(10): p. 2455-2480.
Sifontes, A., et al., Preparación de nanopartículas de plata en ausencia de polimeros estabilizantes. Vol. 33. 2010.
Sperling, R.A. and W.J. Parak, Surface modification, functionalization and bioconjugation of colloidal inorganic nanoparticles. Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, 2010. 368(1915): p. 1333-1383.
Alivisatos, A.P., Semiconductor Clusters, Nanocrystals, and Quantum Dots. Science, 1996. 271(5251): p. 933-937.
Banin, U., et al., Identification of atomic-like electronic states in indium arsenide nanocrystal quantum dots. Nature, 1999. 400: p. 542.
Collier, C.P., et al., Reversible Tuning of Silver Quantum Dot Monolayers Through the Metal-Insulator Transition. Science, 1997. 277(5334): p. 1978-1981.
Kelly, K.L., et al., The optical properties of metal nanoparticles: The influence of size, shape, and dielectric environment. Journal of Physical Chemistry B, 2003. 107, No. 3: p. 668-677.
Pei, Y. and X.C. Zeng, Investigating the structural evolution of thiolate protected gold clusters from first-principles. Nanoscale, 2012. 4(14): p. 4054-4072.
Lv, Y., et al., Preparation of Dialdehyde Chitosan and its Application in Green Synthesis of Silver Nanoparticles. Vol. 8. 2013. 6161-6172.
Sarkany, A., et al., Unsupported Pd nanoparticles prepared by gamma-radiolysis of PdCl2. Solid State Ionics, 2005. 176, No. 1-2: p. 209–215.
G. Nanoparticles: From Theory to Application. 2004: WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Luo, C., et al., The role of poly (ethylene glycol) in the formation of silver nanoparticles. Journal of Colloid and Interface Science, 2005. 288(2): p. 444-448.
Pal, S., Y.K. Tak, and J.M. Song, Does the Antibacterial Activity of Silver Nanoparticles Depend on the Shape of the Nanoparticle? A Study of the Gram-Negative Bacterium em Escherichia coli/em. Applied and Environmental Microbiology, 2007. 73(6): p. 1712-1720.
Raveendran, P., J. Fu, and S.L. Wallen, A simple and “green” method for the synthesis of Au, Ag, and Au–Ag alloy nanoparticles. Green Chemistry, 2006. 8(1): p. 34-38.
Kapoor, S., Preparation, Characterization, and Surface Modification of Silver Particles. Langmuir, 1998. 14(5): p. 1021-1025.
Guozhong, C. Nanostructures and Nanomaterials Imperial College Press, 2004.
